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Poster Session 3

26th International Symposium on Pharmaceutical and Biomedical Analysis (PBA 2015)

July 5-8, 2015

Tbilisi, Georgia

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Poster Session 3

July 8, 2015

14.00-15.00

 

PP-51

Separation of enantiomers of chiral sulfoxides with chloro-substituted tris-phenylcarbamates of cellulose as chiral selectors in high-performance liquid chromatography

Mari Luiza Konjaria1, Natia Shashviashvili1, Rusudan Kakava1, Alessandro Volonterio2, Bezhan Chankvetadze1

1Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

2Dipartimento di Chimica, Materiali ed Ingegneria Chimica "Giulio Natta", Politecnico di Milano, via Mancinelli 720131 Milano, Italy

mari-luiza.konjaria@ens.tsu.edu.ge

 

PP-52

Peptide profiling of internet obtained cerebrolysin using high performance liquid chromatography – electrospray ionization ion trap and ultra-high performance liquid chromatography – ion mobility – quadrupole time of flight mass spectrometry

Bert Gevaert1, Matthias D’Hondt1, Nathalie Bracke1, Han Yao1, Evelien Wynendaele1, Johannes Petrus Cornelis Vissers2, Martin De Cecco2, Jan Claereboudt2, Bart De Spiegeleer1

1Drug Quality and Registration (DruQuaR) group, Faculty of Pharmaceutical Sciences, Ghent University, Ottergemsesteenweg 460, Ghent, B-9000, Belgium

2Waters, ConneXion Business Park, Brusselsesteenweg 500, Zellik, B-1731, Belgium

Bert.Gevaert@UGent.be

 

PP-53

Determination of in-vitro antioxidant capacity of cardiovascular drugs

Yücel Kadioğlu1, Onur Şenol2

1Erzincan University

2Atatürk University

onursenol@atauni.edu.tr

 

PP-54

Quality-by-design risk assessment of topical formulation variability

Lien Taevernier, Sven Detroyer, Lieselotte Veryser, Bart De Spiegeleer

DruQuaR (Drug Quality & Registration) group, Faculty of Pharmaceutical Sciences, Ghent University, Ottergemsesteenweg 460, B-9000 Ghent, Belgium.

Bart.DeSpiegeleer@UGent.be

 

PP-55

The use of UHPLC coupled to single Quad MS detection in franz diffusion cell methodologies

Lieselotte Veryser1, Lien Taevernier1, Nathalie Roche2, Bart De Spiegeleer1,

1DruQuaR (Drug Quality & Registration) group, Faculty of Pharmaceutical Sciences, Ghent University, Ottergemsesteenweg 460, B-9000 Ghent, Belgium.

2Department of Plastic and Reconstructive Surgery, University Hospital Ghent, De Pintelaan 185,   B-9000 Ghent, Belgium.

Bart.DeSpiegeleer@UGent.be

 

PP-56

Forecast electrophoretic behavior of phenolic compounds in terms of capillary zone electrophoresis

Sergey P. Senchenko

Pyatigorsk medico-pharmaceutical institute –branch to Volgograd State Medical University

asp_nauka@mail.ru

 

PP-57

Stability indicating RP-HPLC method development and validation for bosentan in pharmaceutical formulations

Mehmet Emrah Yaman1, Yucel Kadioglu1, DidarTurkan2, Alptug Atila1

1Ataturk University Faculty of Pharmacy Department of Analytical Chemistry, emrahyaman@atauni.edu.tr

 

PP-58

Investigation of HL porphyrin and its Interaction with dsDNA by electrochemical and spectroscopic techniques

Ozge Eren, A.Raşit Çiftaslan, Aysegul Golcu, Mehmet Tumer

Chemistry Department, Kahramanmaras Sutcu Imam University, Kahramanmaras, 46100, Turkey

aysegulgolcu@gmail.com

 

PP-59

Investigation of anticancer activity new metal based drug and comparison with other anticancer agents

Ozge Eren1, Aysegul Golcu1, Ibrahim Demirtas2

1Chemistry Department, Kahramanmaras Sutcu Imam University, Kahramanmaras, 46100, Turkey

2 Department of Chemistry, Cankırı Karatekin University, 18100 Cankırı, Turkey

aysegulgolcu@gmail.com

 

PP-60

Polyphenolic profiles of berries from different Vaccinium species by liquid chromatography coupled with tandem mass spectrometry.

Claudia Ancillotti1, Massimo Del Bubba1, Sandra Furlanetto1

1Department of Chemistry, University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, Florence,

sandra.furlanetto@unifi.it

 

PP-61

Quality by design and mixture-process variable approach in the development of a cyclodextrin-MEEKC method for the assay of diclofenac and its impurities.

Serena Orlandini1, Benedetta Pasquini1, Claudia Caprini1, Vittoria Colotta2, Lucia Squarcialupi2, Massimo Del Bubba1, Sandra Furlanetto1

1Department of Chemistry “U. Schiff”, University of Florence, Via U. Schiff 6-Via della Lastruccia 3, 50019 Sesto F.no, Italy,

2Department of Neuroscience, Psychology, Drug Research and Child Health, Section of
Pharmaceutical and Nutraceutical Sciences, University of Florence, Via U. Schiff 6, 50019 Sesto F.no, Italy

sandra.furlanetto@unifi.it

 

PP-62

Classification of green teas from different geographical origins based on micellar electrokinetic chromatography and chemometric techniques

Benedetta Pasquini1, Mohammad Goodarzi2, Serena Orlandini1, Roberto Gotti3, Claudia Caprini1, Sandra Furlanetto1

1Department of Chemistry “U. Schiff”, University of Florence, Via U. Schiff 6, 50019 Sesto F.no, Italy,

2Laimburg Research Centre for Agriculture and Forestry, Laimburg 6- Pfatten (Vadena), 39040 Auer (Ora), BZ, Italy

3Department of Pharmacy and Biotechnology, University of Bologna, via Belmeloro 6, 40126 Bologna, Italy

sandra.furlanetto@unifi.it

 

PP-63

An analytical quality-by-design approach for a L-asparaginase activity method

Han Yao, Jochem Vancoillie, Matthias D’Hondt, Evelien Wynendaele, Nathalie Bracke, Bart De Spiegeleer

DruQuaR (Drug Quality & Registration) group, Faculty of Pharmaceutical Sciences, Ghent University, Ottergemsesteenweg 460, B-9000 Ghent, Belgium.

Bart.DeSpiegeleer@UGent.be

 

PP-64

Two-dimensional HPLC-FL/MS/MS determination of chiral amino acids in physiological fluids of model mice of ischemic acute kidney injury

Yurika Miyoshi1, Jumpei Sasabe2, Masataka Suzuki2, Yayoi Yonenaga1, Yu Sato1, Maiko Nakane3, Masashi Mita3, Sadakazu Aiso2, Kenji Hamase1

1Graduate School of Pharmaceutical Sciences, Kyushu University, Keio University School of Medicine

3Shiseido Co., Ltd.

miyoshi@phar.kyushu-u.ac.jp

 

PP-65

Development and validation of swab sampling procedure and HPLC method for residual estimation of vincamine

Imeda Rubashvili, Khatuna Loria, Natela Karukhnishvili, Nino Dvali

Aversi-rational Ltd, Quality Control Laboratory,

imeda.rubashvili@aversi

 

PP-66

Evaluation of novel core-shell polysaccharide-based chiral columns for separation of enantiomers of trans –stilbene oxide in high-performance liquid chromatography

Ana Bardavelidze, Teona Ordzhonikidze, Lia Bezitashvili, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

anabardavelidze@yahoo.com

 

PP-67

Evaluation of novel core-shell polysaccharide-based chiral columns for separation of enantiomers of flavanone in high-performance liquid chromatography

Lia Bezitashvili, Ana Bardavelidze, Teona Ordzhonikidze, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

bezhitashvililia@yahoo.com

 

PP-68

Evaluation of novel core-shell polysaccharide-based chiral columns for separation of enantiomers of benzoin in high-performance liquid chromatography

Teona Ordzhonikidze, Ana Bardavelidze, Lia Bezitashvili, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

tekoorjo@mail.ru

 

PP-69

The enantioseparation of chiral phenoxypropionic acid derivatives by HPLC using polysaccharide-based chiral stationary phases and polar-organic mobile phases

Anna Gibradze, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

anukighibradze@yahoo.com

 

PP-70

Enantiomeric analysis of fluorenylmethoxycarbonyl-amino acids by HPLC using the polysaccharide-based chiral columns and polar-organic mobile phases

Nino Ghibradze, Ana Gogolashvili, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

nghibradze@gmail.com

 

PP-71

Qualitative and Quantitative Analysis of Desomorphine Samples by GC/MS

Alexandre Dadianidze, G. Ugulava, Giorgi Kurtsikidze

Forensic-Criminalistic Main Division of the Ministry of Internal Affairs of Georgia

Gulua Street 8, 0114 Tbilisi, Georgia

al.dadianidze@mia.gov.ge

 

PP-72

Enantioseparation of selected chiral organic acids with polysaccharide-based chiral stationary phases and aqueous mobile phases

Iza Matarashvili1, Tamar Khatiashvili1, Darejar Gugunishvili2, Maia Tsintsadze2, Bezhan Chankvetadze1

1Department of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, 0179 Tbilisi, Georgia; iza_matarashvili@mail.ru

2Georgian Technical University, Faculty of Chemical Technology and Metalurgy, Department of Chemical and Biological Technology, Tbilisi, Georgia

iza_matarashvili@mail.ru

 

PP-73

Direct determination of tryptophan and its metabolites in human tears by high performance liquid chromatography

Artur Wnorowski1, Piotr Draczkowski1, Anna Wozniak2, Krzysztof Jozwiak1

1Faculty of Pharmacy, Medical University of Lublin, ul. W. Chodzki 4a, 20-093 Lublin, Poland

2Department of General Ophthalmology, Medical University of Lublin, ul. Chmielna 1 (SPSK Nr 1), 20-079 Lublin, Poland

krzysztof.jozwiak@umlub.pl

 

PP-74

Synthetic analogues of poly [3-(3,4-dihydroxyphenyl)glyceric acid] isolated from comfrey

Maia Merlani1, Vakhtang Barbakadze1, Tamaki Nakano2, Lela Amiranashvili1, Lali Gogilashvili1, Karen Mulkijanyan1, Bezhan Chankvetadze3, Rajesh Agarwal4

1Tbilisi State Medical University I.Kutateladze Institute of Pharmacochemistry, 36 P.Sarajishvili str., Tbilisi, Georgia.

2Catalysis Research Center and Graduate School of Chemical Sciences and Engineering, Hokkaido University, N 21, W 10, Kita-ku, Sapporo 001-0021, Japan.

3Department of Physical and Analytical Chemistry, School of Exact and NaturalSciences, Tbilisi State University, Chavchavadze Ave 1, 0179 Tbilisi, Georgia

4University of Colorado Cancer Center, Aurora, Colorado, USA

maiamer@hotmail.com

PP-75

Study of relationships between enantioselectivity and chemical structure in high-performance liquid chromatography

Rusudan Kakava1, Mari-Luiza Konjaria1, Natia Sahshviashvili1, Alessandro Volonterio2, Bezhan Chankvetadze1

1Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, 179 Tbilisi, Georgia

2Dipartimento di Chimica, Materiali ed Ingegneria Chimica "Giulio Natta", Politecnico di Milano, via Mancinelli 720131 Milano, Italy

rusudan.Kakava@gmail.com

 

PP-76

The enantioseparation of chiral phenoxypropionic acid derivatives by HPLC using polysaccharide-based chiral  stationary phases and polar-organic mobile phases

Nino Ghibradze, Ana Gogolashvili, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

nghibradze@gmail.com

 

PP-77

 

Implementing a design of experiments for chiral separation in SFC: a must?

E. Landagaray1, Y. Zehani2, M. Etaoussi1, S. Yous1, C. Vaccher3, Emanuelle  Lipka2

1Inserm UMR S1172- JPARC- Laboratoire de Chimie Thérapeutique-Faculté de Pharmacie de Lille-59000 France-

2Inserm UMR 995- LIRIC-Laboratoire de Chimie Analytique-Faculté de Pharmacie de Lille-59000 France

3EA 7365 GRITA- Laboratoire de Chimie Analytique-Faculté de Pharmacie de Lille-59000 France

emmanuelle.lipka@univ-lille2.fr