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Poster Session 1

26th International Symposium on Pharmaceutical and Biomedical Analysis (PBA 2015)

July 5-8, 2015

Tbilisi, Georgia

LOGIN / REGISTRATION

Poster Session 1

July 6, 2015

14.00-15.00

 

PP-01

Separation of enantiomers of β-blocker drugs by using polysaccharide-based chiral columns in high-performance liquid chromatography

Antonina Mskhiladze1, Lali Chankvetadze2, Marina Karchkhadze2, Izabela Giuashvili2, Nino Takaishvili2, Natalia Okujava2, Khatuna Gogaladze2, Bezhan Chankvetadze2

1Faculty of Natural Sciences and Healthcare, Sokhumi State University, Polytkovskaya 9, 0186, Tbilisi, Georgia

2Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia

antoninamsxiladze@yahoo.co.uk

 

PP-02

In vitro enantioselective metabolism of tetrabenazine and analysis by capillary electrophoresis

Mariana Zuccherato Bocato1, Anderson Rodrigo Moraes de Oliveira2

1Faculdade de Ciências Farmacêuticas de Ribeirão Preto, Universidade de São Paulo, 14040-903, Ribeirão Preto – SP, Brazil

2Departamento de Química, Faculdade de Filosofia, Ciências e Letras de Ribeirão Preto, Universidade de São Paulo, 14040-901, Ribeirão Preto -SP, Brazil.

deoliveira@usp.br

 

PP-03

Voltammetric determination of entacapone from pharmaceutical dosage forms

Burcin Bozal-Palabiyik, Bengi Uslu

Ankara University Faculty of Pharmacy Department of Analytical Chemistry,

burcinbozal@hotmail.com

 

PP-04

UV-Visible spectrophotometric study of the interaction of aripiprazole with dsDNA

Burcu Dogan-Topal1, Sevinc Kurbanoglu1, Lenka Hlavata2, Jan Labuda2, Sibel A.Ozkan1, Bengi Uslu1

1Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, 06100 Tandogan-Ankara, Turkey,

2Slovak University of Technology, Institute of Analytical Chemistry, Radlinskeho 9, 81237 Bratislava, Slovakia

burcudogan80@yahoo.com, doganb@ankara.edu.tr

 

PP-05

Preparation and evaluation of a 400 µm ID polymer-based HILIC monolithic column with high column efficiency

Chusheng Liu1, Haibin Li1, Jacques Crommen2, Zhengjin Jiang1

1Department of Pharmacy, Jinan University, Guangzhou 510632, China,

2Laboratory of Analytical Pharmaceutical Chemistry, Department of Pharmaceutical Sciences, University of Liege, CHU B36, B-4000 Liege, Belgium,

jzjjackson@hotmail.com

 

PP-06

Flow cytometry: a reliable tool for screening pharmacological compounds targeting P2X7 receptor

Xavier Dezitter1,2, Davy Baudelet2, Germain Homerin2, Amélie Barczyk2, Audrey Vinchent2, Régis Millet2, Emmanuelle Lipka2, Alina Ghinet2, Benoît Rigo2 and Christophe Furman1,2

1Université de Lille 2, Plateforme de binding, ICPAL, F-59000 Lille, France

2Inserm, LIRIC - UMR 995, F-59 000 Lille,

France-emmanuelle.lipka@univ-lille2.fr

 

PP-07

Determination of polyphenols in wines and parts of cluster of autochthonous Georgian white grapes by high-performance liquid chromatography 

Eka Tsutsqiridze1, Nino Beridze1, Izabela Giuashvili1, Lali Chankvetadze1, Armaz Shalashvili2, Bezhan Chankvetadze1

1Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia,

2Agricultural University of Georgia, 240, David Aghmashenebeli Alley, 0159 Tbilisi, Georgia

ekacucqiridze@yahoo.com

 

PP-08

Enantiomer elution order of chiral dihydropyridine derivatives with polysaccharide-based chiral stationary phases and normal-phase eluents in high-performance liquid chromatography

Elene Sordia, Bezhan Chankvetadze

Department of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

elenekusa@gmail.com

 

PP-09

Voltammetric analysis of hydrocortisone using a glassy carbon electrode

Ertugrul Keskin1, Yavuz Yardım2, Abdulkadir Levent3, Zühre Şentürk4

1Adıyaman Univ., Fac. of Pharmacy, Dept. of Anal. Chem., 02040 Adıyaman, Turkey

2Yüzüncü Yıl Univ., Fac. of Pharmacy, Dept. of Anal. Chem., 65080 Van, Turkey

3Batman Univ., Vocational School of Health Services, 72100 Batman, Turkey

4Yüzüncü Yıl Univ., Faculty of Sci., Dept. of Anal. Chem., 65080 Van, Turkey

keskinertugrul@yahoo.com

 

PP-10

Evaluation of highly sulfated maltodextrin as a novel anionic chiral selector

Hadi Tabani1, Kamal Khodaei1, Yasamin Bide2, Farzaneh Dorabadi Zare2, Ali Reza Fakhari2

1Department of Environmental Geology, Research Institute of Applied Sciences (ACECR),

Shahid Beheshti University, Tehran, Iran

2Department of pure Chemistry, Faculty of Chemistry, Shahid Beheshti University, G. C., P.O. Box 19396-4716, Evin, Tehran, Iran

farzaneh_dorabadi@yahoo.com

 

PP-11

High-performance liquid chromatographic separations of stereoisomers of chiral basic agrochemicals with polysaccharide-based chiral columns and polar organic mobile phases

Iza Matarashvili1, Iamze Shvangiradze2, Lali Chankvetadze1, Shota Sidamonidze1,2, Nino Takaishvili1, Bezhan Chankvetadze1

1Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, 0179 Tbilisi, Georgia

2Department of Ecology and Environmental Protection, Faculty of Informatics, Mathematics and Natural Sciences, Georgian University of St. Andrew the Apostle, Chavchavadze Ave 53 A, 0162 Tbilisi, Georgia

Iza_matarashvili@mail.ru, iashvangiradze@yahoo.com

 

PP-12

HPLC separation of enantiomers of some chiral carboxylic acid derivatives using polysaccharide-based chiral columns and polar organic mobile phases

Iza Matarashvili, Lali Chankvetadze, Bezhan Chankvetadze

Department of Physical and Analytical Chemistry, School of Exact and Natural Sciences,   Tbilisi State University, Chavchavadze Ave 3, 0179 Tbilisi, Georgia

Iza_matarashvili@mail.ru

 

PP-13

Determination of monophenolics in red dessert wines produced with different maceration techniques

Inessa A. Kekelidze1, Nana V. Ebelashvili1,   Lali G. Chankvetadze2, Murman Sh. Japaridze1 

1Agricultural University of Georgia,

2Ivane Javakhishvili Tbilisi State University

inessakekelidze@yahoo.com

 

PP-14

Characterization and comparison of water soluble polysaccharides from Lycium barbarum (wolfberry) in China using saccharide mapping and HPSEC-MALLS-RID with the refractive index increment

Jing Zhao, Ding-Tao Wu, Shao-Ping Li

State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao, China,

jingzhao@umac.mo

 

PP-15

Analysis of negatively charged cyclodextrins on different stationary phases: combination of ion-exchange and complex forming interactions

Julianna Szemán1, Róbert Iványi2, Krisztina Ludányi3, Borbála Dalmadi-Kiss3, Lajos Szente1, Gyula Vígh4

1CycloLab Ltd., Budapest, Hungary,

2Bio-Sol-Dex Ltd., Kecskemét, Hungary

3Semmelweis University, Department of Pharmaceutics, Hungary

4Texas A&M University, Department of Chemistry, College Station, USA

szeman.j@cyclolab.hu

 

PP-16

The effect of basic and acidic additives on separation of beta-blocker enantiomers on polysaccharide-based chiral columns and acetonitrile as mobile phase

Khatuna Gogaladze, Lali Chankvetadze, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 1, 0179 Tbilisi, Georgia

Khat78@gmail.com

 

PP-17

Determination of sulfonamides in chicken muscle and eggs By QuEChERS combined with HPLC AND photo induced fluorescence detection

José Fernando Huertas-Pérez1, Natalia Arroyo-Manzanares1, Lucie Havlíková2, Laura Gámiz-Gracia1, Petr Solich2, Ana M. García-Campaña1

1Department of Analytical Chemistry, Faculty of Sciences, University of Granada,

Campus Fuentenueva s/n, E-18071 Granada, Spain

2Department of Analytical Chemistry, Faculty of Pharmacy, Charles University in Prague,

Heyrovského 1203, 500 05 Hradec Králové, Czech Republic.

havlikova@faf.cuni.cz

 

PP-18

Quantitative determination of phenolic compounds in the white wine Tsinandali produced by different manufacturers

Megi Choniashvili, Eka Tsutsqiridze, Bezhan Chankvetadze.

Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia,

megi.choniashvili@yahoo.com

 

PP-19

Enantioseparation of chiral antimycotic drugs on polysaccharide-based chiral columns in polar-organic and reversed- phase high-performance liquid chromatography

Marina Karchkhadze1, Antonina Mskhiladze 1, 2, Lali Chankvetadze 1, Aleksandre

Dadianidze1, Bezhan Chankvetadze 1

1Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, 179 Tbilisi, Georgia

2Faculty of Natural Sciences and Healthcare, Sokhumi State University, Polytkovskaya 9, 0186, Tbilisi, Georgia

karchkhadze.marina@yahoo.com

 

PP-20

Evaluation of selected cell receptors of preserved blood for specialist biocompatibility study

Magdalena Kościelniak-Ziemniak, Maciej Gawlikowski, Roman Kustosz, Malgorzata Gonsior

Foundation of Cardiac Surgery Development, Artificial Heart Laboratory, 345a Wolności Street, 41-800 Zabrze, Poland,

mkoscielniak_ziemniak@frk.pl

 

PP-21

Application of electron paramagnetic resonance spectroscopy to determine concentration of thermally formed free radicals in exemplary drugs

Magdalena Kościelniak-Ziemniak1, 2, Barbara Pilawa2

1Foundation of Cardiac Surgery Development, 345a Wolności Street, 41-800 Zabrze, Poland,

2Department of Biophysics, School of Pharmacy and Division of Laboratory Medicine in Sosnowiec, Medical University of Silesia, Jedności 8, 41-200 Sosnowiec, Poland

megdy@interia.pl

 

PP-22

EPR studies of spin-spin and spin-lattice relaxation in heated glucocorticosteroides

Magdalena Kościelniak-Ziemniak1, 2, Barbara Pilawa2

1Foundation of Cardiac Surgery Development, 345a Wolności Street, 41-800 Zabrze, Poland,

2Department of Biophysics, School of Pharmacy and Division of Laboratory Medicine in Sosnowiec, Medical University of Silesia,  8 Jedności Street, 41-200 Sosnowiec, Poland

megdy@interia.pl

 

PP-23

Optimization and validation of a RP-LC method for the sensitive determination of antazoline and tetrahydrozoline

Mehmet Gumustas, Bengi Uslu, Sibel A. Ozkan

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey

mgumustas@hotmail.com

 

PP-24

Determination of emtricitabine, rilpivirine and tenofovir from biological samples with using LC and CE methods

Mehmet Gumustas, M. Gokhan Caglayan, Feyyaz Onur, Sibel A. Ozkan

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey

mgumustas@hotmail.com

 

PP-25

Determination of polyphenols in wines and parts of cluster of autochthonous Georgian red grapes by high-performance liquid chromatography 

Nina Beridze1, Eka Tsutsqiridze1, Izabela Giuashvili1, Lali Chankvetadze1, Armaz Shalashvili2, Bezhan Chankvetadze1

1Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia

2Agricultural University of Georgia, 240, David Aghmashenebeli Alley, 0159 Tbilisi, Georgia

niniberidze23@yahoo.com