July 6, 2015

14.00-15.00

PP-01

Separation of enantiomers of β-blocker drugs by using polysaccharide-based chiral columns in high-performance liquid chromatography

Antonina Mskhiladze¹, Lali Chankvetadze², Marina Karchkhadze², Izabela Giuashvili², Nino Takaishvili², Natalia Okujava², Khatuna Gogaladze², Bezhan Chankvetadze²

¹Faculty of Natural Sciences and Healthcare, Sokhumi State University, Polytkovskaya 9, 0186, Tbilisi, Georgia

²Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia

antoninamsxiladze@yahoo.co.uk

PP-02

In vitro enantioselective metabolism of tetrabenazine and analysis by capillary electrophoresis

Mariana Zuccherato Bocato¹, Anderson Rodrigo Moraes de Oliveira²

¹Faculdade de Ciências Farmacêuticas de Ribeirão Preto, Universidade de São Paulo, 14040-903, Ribeirão Preto – SP, Brazil

²Departamento de Química, Faculdade de Filosofia, Ciências e Letras de Ribeirão Preto, Universidade de São Paulo, 14040-901, Ribeirão Preto -SP, Brazil.

deoliveira@usp.br

PP-03

Voltammetric determination of entacapone from pharmaceutical dosage forms

Burcin Bozal-Palabiyik, Bengi Uslu

Ankara University Faculty of Pharmacy Department of Analytical Chemistry,

burcinbozal@hotmail.com

PP-04

UV-Visible spectrophotometric study of the interaction of aripiprazole with dsDNA

Burcu Dogan-Topal¹, Sevinc Kurbanoglu¹, Lenka Hlavata², Jan Labuda², Sibel A.Ozkan¹, Bengi Uslu¹

¹Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, 06100 Tandogan-Ankara, Turkey,

²Slovak University of Technology, Institute of Analytical Chemistry, Radlinskeho 9, 81237 Bratislava, Slovakia

burcudogan80@yahoo.com, doganb@ankara.edu.tr

PP-05

Preparation and evaluation of a 400 µm ID polymer-based HILIC monolithic column with high column efficiency

Chusheng Liu¹, Haibin Li¹, Jacques Crommen², Zhengjin Jiang¹

¹Department of Pharmacy, Jinan University, Guangzhou 510632, China,

²Laboratory of Analytical Pharmaceutical Chemistry, Department of Pharmaceutical Sciences, University of Liege, CHU B36, B-4000 Liege, Belgium,

jzjjackson@hotmail.com

PP-06

Flow cytometry: a reliable tool for screening pharmacological compounds targeting P2X7 receptor

Xavier Dezitter^1,2, Davy Baudelet², Germain Homerin², Amélie Barczyk², Audrey Vinchent², Régis Millet², Emmanuelle Lipka², Alina Ghinet², Benoît Rigo² and Christophe Furman^1,2

¹Université de Lille 2, Plateforme de binding, ICPAL, F-59000 Lille, France

²Inserm, LIRIC - UMR 995, F-59 000 Lille,

France-emmanuelle.lipka@univ-lille2.fr

PP-07

Determination of polyphenols in wines and parts of cluster of autochthonous Georgian white grapes by high-performance liquid chromatography 

Eka Tsutsqiridze¹, Nino Beridze¹, Izabela Giuashvili¹, Lali Chankvetadze¹, Armaz Shalashvili², Bezhan Chankvetadze¹

¹Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia,

²Agricultural University of Georgia, 240, David Aghmashenebeli Alley, 0159 Tbilisi, Georgia

ekacucqiridze@yahoo.com

PP-08

Enantiomer elution order of chiral dihydropyridine derivatives with polysaccharide-based chiral stationary phases and normal-phase eluents in high-performance liquid chromatography

Elene Sordia, Bezhan Chankvetadze

Department of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, Tbilisi 0179, Georgia

elenekusa@gmail.com

PP-09

Voltammetric analysis of hydrocortisone using a glassy carbon electrode

Ertugrul Keskin¹, Yavuz Yardım², Abdulkadir Levent³, Zühre Şentürk⁴

¹Adıyaman Univ., Fac. of Pharmacy, Dept. of Anal. Chem., 02040 Adıyaman, Turkey

²Yüzüncü Yıl Univ., Fac. of Pharmacy, Dept. of Anal. Chem., 65080 Van, Turkey

³Batman Univ., Vocational School of Health Services, 72100 Batman, Turkey

⁴Yüzüncü Yıl Univ., Faculty of Sci., Dept. of Anal. Chem., 65080 Van, Turkey

keskinertugrul@yahoo.com

PP-10

Evaluation of highly sulfated maltodextrin as a novel anionic chiral selector

Hadi Tabani¹, Kamal Khodaei¹, Yasamin Bide², Farzaneh Dorabadi Zare², Ali Reza Fakhari²

¹Department of Environmental Geology, Research Institute of Applied Sciences (ACECR),

Shahid Beheshti University, Tehran, Iran

²Department of pure Chemistry, Faculty of Chemistry, Shahid Beheshti University, G. C., P.O. Box 19396-4716, Evin, Tehran, Iran

farzaneh_dorabadi@yahoo.com

PP-11

High-performance liquid chromatographic separations of stereoisomers of chiral basic agrochemicals with polysaccharide-based chiral columns and polar organic mobile phases

Iza Matarashvili¹, Iamze Shvangiradze², Lali Chankvetadze¹, Shota Sidamonidze^1,2, Nino Takaishvili¹, Bezhan Chankvetadze¹

¹Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, 0179 Tbilisi, Georgia

²Department of Ecology and Environmental Protection, Faculty of Informatics, Mathematics and Natural Sciences, Georgian University of St. Andrew the Apostle, Chavchavadze Ave 53 A, 0162 Tbilisi, Georgia

Iza_matarashvili@mail.ru, iashvangiradze@yahoo.com

PP-12

HPLC separation of enantiomers of some chiral carboxylic acid derivatives using polysaccharide-based chiral columns and polar organic mobile phases

Iza Matarashvili, Lali Chankvetadze, Bezhan Chankvetadze

Department of Physical and Analytical Chemistry, School of Exact and Natural Sciences,   Tbilisi State University, Chavchavadze Ave 3, 0179 Tbilisi, Georgia

Iza_matarashvili@mail.ru

PP-13

Determination of monophenolics in red dessert wines produced with different maceration techniques

Inessa A. Kekelidze¹, Nana V. Ebelashvili¹,   Lali G. Chankvetadze², Murman Sh. Japaridze¹ 

¹Agricultural University of Georgia,

²Ivane Javakhishvili Tbilisi State University

inessakekelidze@yahoo.com

PP-14

Characterization and comparison of water soluble polysaccharides from Lycium barbarum (wolfberry) in China using saccharide mapping and HPSEC-MALLS-RID with the refractive index increment

Jing Zhao, Ding-Tao Wu, Shao-Ping Li

State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao, China,

jingzhao@umac.mo

PP-15

Analysis of negatively charged cyclodextrins on different stationary phases: combination of ion-exchange and complex forming interactions

Julianna Szemán¹, Róbert Iványi², Krisztina Ludányi³, Borbála Dalmadi-Kiss³, Lajos Szente¹, Gyula Vígh⁴

¹CycloLab Ltd., Budapest, Hungary,

²Bio-Sol-Dex Ltd., Kecskemét, Hungary

³Semmelweis University, Department of Pharmaceutics, Hungary

⁴Texas A&M University, Department of Chemistry, College Station, USA

szeman.j@cyclolab.hu

PP-16

The effect of basic and acidic additives on separation of beta-blocker enantiomers on polysaccharide-based chiral columns and acetonitrile as mobile phase

Khatuna Gogaladze, Lali Chankvetadze, Bezhan Chankvetadze

Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 1, 0179 Tbilisi, Georgia

Khat78@gmail.com

PP-17

Determination of sulfonamides in chicken muscle and eggs By QuEChERS combined with HPLC AND photo induced fluorescence detection

José Fernando Huertas-Pérez¹, Natalia Arroyo-Manzanares¹, Lucie Havlíková², Laura Gámiz-Gracia¹, Petr Solich², Ana M. García-Campaña¹

¹Department of Analytical Chemistry, Faculty of Sciences, University of Granada,

Campus Fuentenueva s/n, E-18071 Granada, Spain

²Department of Analytical Chemistry, Faculty of Pharmacy, Charles University in Prague,

Heyrovského 1203, 500 05 Hradec Králové, Czech Republic.

havlikova@faf.cuni.cz

PP-18

Quantitative determination of phenolic compounds in the white wine Tsinandali produced by different manufacturers

Megi Choniashvili, Eka Tsutsqiridze, Bezhan Chankvetadze.

Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia,

megi.choniashvili@yahoo.com

PP-19

Enantioseparation of chiral antimycotic drugs on polysaccharide-based chiral columns in polar-organic and reversed- phase high-performance liquid chromatography

Marina Karchkhadze¹, Antonina Mskhiladze ^{1, 2}, Lali Chankvetadze ¹, Aleksandre

Dadianidze¹, Bezhan Chankvetadze ¹

¹Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Chavchavadze Ave 3, 179 Tbilisi, Georgia

²Faculty of Natural Sciences and Healthcare, Sokhumi State University, Polytkovskaya 9, 0186, Tbilisi, Georgia

karchkhadze.marina@yahoo.com

PP-20

Evaluation of selected cell receptors of preserved blood for specialist biocompatibility study

Magdalena Kościelniak-Ziemniak, Maciej Gawlikowski, Roman Kustosz, Malgorzata Gonsior

Foundation of Cardiac Surgery Development, Artificial Heart Laboratory, 345a Wolności Street, 41-800 Zabrze, Poland,

mkoscielniak_ziemniak@frk.pl

PP-21

Application of electron paramagnetic resonance spectroscopy to determine concentration of thermally formed free radicals in exemplary drugs

Magdalena Kościelniak-Ziemniak^{1, 2}, Barbara Pilawa²

¹Foundation of Cardiac Surgery Development, 345a Wolności Street, 41-800 Zabrze, Poland,

²Department of Biophysics, School of Pharmacy and Division of Laboratory Medicine in Sosnowiec, Medical University of Silesia, Jedności 8, 41-200 Sosnowiec, Poland

megdy@interia.pl

PP-22

EPR studies of spin-spin and spin-lattice relaxation in heated glucocorticosteroides

Magdalena Kościelniak-Ziemniak^{1, 2}, Barbara Pilawa²

¹Foundation of Cardiac Surgery Development, 345a Wolności Street, 41-800 Zabrze, Poland,

²Department of Biophysics, School of Pharmacy and Division of Laboratory Medicine in Sosnowiec, Medical University of Silesia,  8 Jedności Street, 41-200 Sosnowiec, Poland

megdy@interia.pl

PP-23

Optimization and validation of a RP-LC method for the sensitive determination of antazoline and tetrahydrozoline

Mehmet Gumustas, Bengi Uslu, Sibel A. Ozkan

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey

mgumustas@hotmail.com

PP-24

Determination of emtricitabine, rilpivirine and tenofovir from biological samples with using LC and CE methods

Mehmet Gumustas, M. Gokhan Caglayan, Feyyaz Onur, Sibel A. Ozkan

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey

mgumustas@hotmail.com

PP-25

Determination of polyphenols in wines and parts of cluster of autochthonous Georgian red grapes by high-performance liquid chromatography 

Nina Beridze¹, Eka Tsutsqiridze¹, Izabela Giuashvili¹, Lali Chankvetadze¹, Armaz Shalashvili², Bezhan Chankvetadze¹

¹Institute of Physical and Analytical Chemistry, Faculty of Exact and Natural Sciences, Ivane Javakhishvili Tbilisi State University, 3,  I. Chavchavadze Ave., 0179 Tbilisi, Georgia

²Agricultural University of Georgia, 240, David Aghmashenebeli Alley, 0159 Tbilisi, Georgia

niniberidze23@yahoo.com